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CMMP Scanning Electron Microscopy

CMMP Scanning Electron Microscopy. Wednesday, January 7, 2015. The Choice of Beam Energy: The Letter "a". In the second image, taken at 10 kV, small amorphous blobs of fused toner start to become visible, especially on some of the larger flat fibers. Nevertheless, it's largely impossible to make out the "a" letter. Labels: back scattered electrons. Tuesday, January 6, 2015. The final micrograph shows the edge of the tube at high tilt. The large depth of field at large working distance allows one to s...

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CMMP Scanning Electron Microscopy. Wednesday, January 7, 2015. The Choice of Beam Energy: The Letter a. In the second image, taken at 10 kV, small amorphous blobs of fused toner start to become visible, especially on some of the larger flat fibers. Nevertheless, it's largely impossible to make out the a letter. Labels: back scattered electrons. Tuesday, January 6, 2015. The final micrograph shows the edge of the tube at high tilt. The large depth of field at large working distance allows one to s...
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CMMP Scanning Electron Microscopy | sem-cmmp.blogspot.com Reviews

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CMMP Scanning Electron Microscopy. Wednesday, January 7, 2015. The Choice of Beam Energy: The Letter "a". In the second image, taken at 10 kV, small amorphous blobs of fused toner start to become visible, especially on some of the larger flat fibers. Nevertheless, it's largely impossible to make out the "a" letter. Labels: back scattered electrons. Tuesday, January 6, 2015. The final micrograph shows the edge of the tube at high tilt. The large depth of field at large working distance allows one to s...

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CMMP Scanning Electron Microscopy: Which Beam Energy Should I Use?

http://www.sem-cmmp.blogspot.com/2013/06/which-beam-energy-should-i-use.html

CMMP Scanning Electron Microscopy. Saturday, June 1, 2013. Which Beam Energy Should I Use? Dropping the beam energy 10 keV is shown in the second image. It's clearly the same structure- but it is slightly nuanced. The electron range. Is significantly less at 10 keV, even in a low density matrix like activated charcoal. This results in the enhancement of edge effects. So, which is correct? They all are. The SEM isn't lying. Which is best? Labels: back scattered electrons. Subscribe to: Post Comments (Atom).

2

CMMP Scanning Electron Microscopy: Field Emission SEM

http://www.sem-cmmp.blogspot.com/2012/10/field-emission-sem.html

CMMP Scanning Electron Microscopy. Friday, October 5, 2012. This is an image of the Au cluster on HPOG standard used to check the resolution of the JEOL 5900 SEM. This image was taken using an FEI Nova 400 field-emission FESEM in the FSU BSIR. A comparison can be made with an image taken with the JEOL 5900 in a previous post. SEM's and FESEM's are different instruments with unique capabilities and limitations. For more information about the BSIR FE SEM look here. Subscribe to: Post Comments (Atom).

3

CMMP Scanning Electron Microscopy: The Choice of Beam Energy: The Letter "a"

http://www.sem-cmmp.blogspot.com/2015/01/the-choice-of-beam-energy-letter-a.html

CMMP Scanning Electron Microscopy. Wednesday, January 7, 2015. The Choice of Beam Energy: The Letter "a". In the second image, taken at 10 kV, small amorphous blobs of fused toner start to become visible, especially on some of the larger flat fibers. Nevertheless, it's largely impossible to make out the "a" letter. Labels: back scattered electrons. Subscribe to: Post Comments (Atom). The Choice of Beam Energy: The Letter a. I manage the analytical and fabrication tools in the Condensed Matter and Materia...

4

CMMP Scanning Electron Microscopy: EDS Detector Window Absorption

http://www.sem-cmmp.blogspot.com/2012/04/eds-detector-window-absorption.html

CMMP Scanning Electron Microscopy. Thursday, April 12, 2012. EDS Detector Window Absorption. This graph shows the transmission through several different EDS detector windows. The solid line is for the Moxtek AP1.3, the dot-dashed line for the Moxtek HT2.2 and the dashed line for the Moxtek AP3.3. Our EDS detector has an AP3.3 window. The graph is borrowed from F. Scholze and M. Procop, X-Ray Spectrom. Subscribe to: Post Comments (Atom). Beam Energy and Topography: SE1 and SE2. Kaersutite: Low Energy EDS.

5

CMMP Scanning Electron Microscopy: AuPd Sputter Coater Calibration

http://www.sem-cmmp.blogspot.com/2012/07/aupd-sputter-coater-calibration.html

CMMP Scanning Electron Microscopy. Monday, July 30, 2012. AuPd Sputter Coater Calibration. In coating for SEM applications, the first choice is materials. AuPd is the ideal choice for imaging. Because of the small AuPd grains. For spectroscopic applications. The high density of AuPd will attenuate X-rays- particularly low-energy X-rays. In such applications a flash coating of graphite is desirable. AuPd coating is done according to recipe. The following parameters are considered fixed. AuPd Coating Proce...

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CMMP Scanning Probe Microscopy: Flattening & Flattening Artifacts

http://spm-cmmp.blogspot.com/2011/06/flattening-flattening-artifacts.html

CMMP Scanning Probe Microscopy. Thursday, June 30, 2011. Flattening and Flattening Artifacts. AFM images generally require some post-processing. One method of post-processing is flattening. In this case a polynomial of order n. Is fit and subtracted from every trace and retrace. It is called "flattening" because this method of processing tends to flatten or unroll an AFM image. It is also a potential source of artifacts. To remedy these artifacts stop bands. Grains on a film surface. In these applica...

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CMMP Scanning Probe Microscopy: Magnetic Force Microscopy

http://spm-cmmp.blogspot.com/2011/06/magnetic-force-microscopy.html

CMMP Scanning Probe Microscopy. Monday, June 20, 2011. The force exerted on a dipole is the dot product of the dipole moment and the gradient of the field at the surface. In magnetic force microscopy. MFM- these dipole magnetic forces are detected as a change in cantilever phase and amplitude a finite distance above the surface. In an MFM image, the tip is tapped on the surface. To measure the surface morphology, and then rescanned across the surface 50-150 nm above the surface. Fast MFM in Contact Mode.

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CMMP Ellipsometry: Gaertner Ellipsometer

http://ellip-cmmp.blogspot.com/2011/06/gaertner-ellipsometer.html

Friday, June 17, 2011. The CMMP group at the Florida State University Department of Physics has a Gaertner L116B ellipsometer that is available to the local research community. There are no fees for use of this instrument. Fast; non-contact; cost; ideal for Si oxides and nitrides; ideal for materials with well known optical properties for HeNe visible radiation. Subscribe to: Post Comments (Atom). View my complete profile. CMMP Scanning Electron Microscopy. CMMP Scanning Probe Microscopy.

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CMMP Magneto-Transport

http://mt-cmmp.blogspot.com/2013/10/these-are-optical-photos-of-ppms.html

Friday, October 25, 2013. These are optical photos of the PPMS resistivity pucks. The CMMP group has three of these so that samples can be contacted while one is in the system. Each puck has three stations that include four contacts for transport measurements. These contacts can be accessed either by our break-out box or the PPMS controller's resistivity bridge depending upon the application. Contacting samples is an art, and CMMP will not do that for you. The availability of three sets of contacts, labe...

overview-cmmp.blogspot.com overview-cmmp.blogspot.com

CMMP User Facilities: October 2014

http://overview-cmmp.blogspot.com/2014_10_01_archive.html

Wednesday, October 1, 2014. Because of staffing limitations at the CMMP facility, services requiring CMMP staff may involve some delay as instruments and staff time become available. In general, services are provided on a first-come, first server basis. This rule is subject to the discretion of the facility manager according to the availability of instrumentation, staffing, etc. The entries in italics. Are set as high priority, and the projects in red. Are either currently underway or scheduled.

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CMMP User Facilities: June 2013

http://overview-cmmp.blogspot.com/2013_06_01_archive.html

Sunday, June 30, 2013. Users of the CMMP facilities are requested to recognize the Florida State University Department of Physics Condensed Matter and Material Physics (CMMP) user facility in publications using this lab as a resource. While journal article co-authorship is not required to use the CMMP facilities, please consider offering co-authorship to CMMP staff contributing beyond the scope of routine instrument training and consultation. Subscribe to: Posts (Atom). View my complete profile.

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CMMP User Facilities: Introduction

http://overview-cmmp.blogspot.com/2012/04/introduction.html

Friday, July 5, 2013. Vibrating sample magnetometry, dielectric spectroscopy. And PPMS for magneto-transport measurements. Scanning electron microscopy (SEM with EDS). Scanning probe microscopy (SPM). X-ray photoelectron spectroscopy (XPS). Scanning probe microscopy (SPM). Evaporation, sputtering, UHV sputtering. Dip-pen nanolithography (DPN), photolithography, e-beam lithography, wet etching, reactive ion etching (RIE), ion milling, plasma etching, wire bonder, class 1000 cleanroom.

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CMMP SQUID Magnetometry: SQUID Drift

http://squid-cmmp.blogspot.com/2011/07/squid-drift.html

Tuesday, July 5, 2011. The SQUID profiles- the SQUID device output voltage vs. Extraction distance- are generally detrended. To remove any background on the SQUID profile. This occurs automatically, but one can inspect the raw SQUID voltages through the diagnostic menus of the MultiVu software. It is not unusual to see the SQUID voltage run through its output range repeatedly as the SQUID amplifier's gain is reset again and again. This is due the effect of SQUID drift. Shows M vs. t. For the magnet being...

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CMMP Scanning Probe Microscopy: Tapping AFM of Buckypaper

http://spm-cmmp.blogspot.com/2011/06/tapping-afm-of-buckypaper.html

CMMP Scanning Probe Microscopy. Tuesday, June 21, 2011. Tapping AFM of Buckypaper. This image is a tapping AFM image performed on a Buckypaper sample made of carbon nanotube bundles precipitated into a fibrous paper. Even though the system consists of free-standing fibers with very deep pores, it could be easily imaged. Subscribe to: Post Comments (Atom). Plane Fitting and Bow Artifacts. Flattening and Flattening Artifacts. Image Artifact: Self-Similar Triangles. Fast MFM in Contact Mode.

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CMMP Scanning Electron Microscopy

CMMP Scanning Electron Microscopy. Wednesday, January 7, 2015. The Choice of Beam Energy: The Letter "a". In the second image, taken at 10 kV, small amorphous blobs of fused toner start to become visible, especially on some of the larger flat fibers. Nevertheless, it's largely impossible to make out the "a" letter. Labels: back scattered electrons. Tuesday, January 6, 2015. The final micrograph shows the edge of the tube at high tilt. The large depth of field at large working distance allows one to s...

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